Synthesis of substituted norbornenes and their ...



Title Synthesis of substituted norbornenes and their polymerization to polynorbornenes with flexible aliphatic side-chains.
Author(s) Alaa S. Abd-El-Aziz, Leslie J. May, Andrea L. Edel
Journal Macromolecular Rapid Communications,
Date 2000
Volume 21
Issue 9
Start page 598
End page 602
Abstract Synthesis and characterization of new thermally stable polynorbornenes functionalized with pendent flexible side-chains are reported. The flexible side-chains with terminal hydroxy groups were synthesized via SNAr reactions of cyclopentadienyliron-complexed chlorobenzenes with aliphatic diols. Condensation of these side-chains with exo,endo-5-norbornene-2-carboxylic acid led to the formation of substituted monomers which were characterized using one- and two-dimensional NMR techniques. Ring-opening metathesis polymerization of these monomers yielded polynorbornenes with pendent side-chains.
DOI 10.1002/1521-3927(20000601)21:9<598::AID-MARC598>3.0.CO;2-0,

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