Kinetics analysis of degradation of polynorbornene ...

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Title Kinetics analysis of degradation of polynorbornene containing aryl or hetaryl azo dye
Author(s) A. A. Joraid, A. A. Abu-Sehly, S. N. Alamri, S. Y. Al-Raqa, P. O. Shipman, P. R. Shipley, A. S. Abd-El-Aziz
Journal Thermochimica Acta,
Date 2012
Volume 529
Issue
Start page 22
End page 24
Abstract The Vyazovkin model-free method were applied to study non-isothermal degrdn. of an aryl and hetaryl azo dye-contg. polynorbornene using a differential scanning calorimetric (DSC) technique. The samples were heated in nitrogen, with heating rates in the range 5-50 K min-1. The isoconversional method of Vyazovkin was used to det. the variation of the activation energy for degrdn. with temp., E α(T). The values of E α(T) were found to be almost independent of temp. The results of isoconversional methods used suggest that the transition follows a single-step kinetics reaction mechanism. [on SciFinder(R)]
DOI 10.1016/j.tca.2011.11.007

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