Intercalation of tetraazamacrocycles into molybdenum ...

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Title Intercalation of tetraazamacrocycles into molybdenum disulfide
Author(s) Rabin Bissessur, Robert I. Haines, R. Bruning
Journal Journal of Materials Chemistry
Date 2003
Volume 13
Issue 1
Start page 44
End page 49
Abstract A series of intercalation compounds of tetraazamacrocycles in molybdenum disulfide have been synthesized using the exfoliation and restacking properties of LiMoS2. The sandwiched compounds were characterized by powder X-ray diffraction, thermogravimetric analyses, differential scanning calorimetry, and four-probe electrical conductivity measurements. The interlayer spacing of the intercalation compound was found to be dependent on the size of the macrocyclic ligand, indicating that the intercalated macrocycles are co-planar with the MoS2 sheets.
DOI 10.1039/B208237N
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