Intercalation of tetraazamacrocycles into molybdenum ...



Title Intercalation of tetraazamacrocycles into molybdenum disulfide
Author(s) Rabin Bissessur, Robert I. Haines, R. Bruning
Journal Journal of Materials Chemistry
Date 2003
Volume 13
Issue 1
Start page 44
End page 49
Abstract A series of intercalation compounds of tetraazamacrocycles in molybdenum disulfide have been synthesized using the exfoliation and restacking properties of LiMoS2. The sandwiched compounds were characterized by powder X-ray diffraction, thermogravimetric analyses, differential scanning calorimetry, and four-probe electrical conductivity measurements. The interlayer spacing of the intercalation compound was found to be dependent on the size of the macrocyclic ligand, indicating that the intercalated macrocycles are co-planar with the MoS2 sheets.
DOI 10.1039/B208237N
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