Synthesis and x-ray crystal structure of ...

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Title Synthesis and x-ray crystal structure of meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di- (1-methyl-naphthalene).
Author(s) Robert I. Haines, D. R. Hutchings
Journal Molecules
Date 2003
Volume 8
Issue 2
Start page 243
End page 250
Abstract The pendant-arm macrocycle, meso-5,5,7,12,12,14-hexamethy 1,4,8,11-tetraazacyclotetradecane- 1,8-di-(1-methylnaphthalene) has been synthesized and its single crystal structure determined. The molecule crystallizes in a primitive monoclinic cell, with the space group P2(1)/a (#14). The cell dimensions are a = 10.778(3)Angstrom, b = 13.809(3) Angstrom, c = 11.420(2) Angstrom, There Exists = 102.49(2)degrees, volume = 1659.5(6) Angstrom(3).
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